EmissionsLookup
Non-Compliance TRI Reporter Clean Air Act Clean Water Act RCRA

3M CHEMICAL OPERATIONS' COTTAGE GROVE FACILITY

Quick Summary

  • Released 777,126 lbs of toxic chemicals to the environment in the most recent TRI reporting year.
  • Currently out of compliance in at least one environmental program (CAA, CWA, or RCRA).
  • Assessed $3,123,859 in total penalties since records began.
  • Reports releases of PFAS ("forever chemicals").
  • Reports releases of chemicals classified as known or probable carcinogens.
Address
10746 INNOVATION RD
COTTAGE GROVE, MN 55016
View on map ↗
County
WASHINGTON County
Industry
Manufacturing
NAICS (North American Industry Classification)
325998
Inspections
21 · last May 20, 2025
Total Penalties
$3,123,859 · last Feb 7, 2024
Registry ID
110000423667

How This Compares

#4 of 421 TRI reporters in MN
#259 of 16,877 TRI reporters in Manufacturing

Ranked by most recent year's total TRI releases.

Compliance Status (Last 12 Quarters)

Number of calendar quarters, out of the last 12, in which this facility was in violation of its permit. Zero means no recorded violations in that program over the past three years.

1
Air (CAA)
Qtrs Non-Compliant
7
Water (CWA)
Qtrs Non-Compliant
12
Hazardous Waste (RCRA)
Qtrs Non-Compliant

TRI Toxic Chemical Releases

Annual pounds of each toxic chemical released to air, water, and land, as reported to the EPA Toxic Release Inventory. Carcinogen (♦) and PFAS designations are per EPA and IARC classifications.

Emissions Trend (2015–2024) -45% overall
Year Total Releases (lbs) vs Prior Year
2015 815,088
2016 936,409 +15%
2017 777,126 -17%
2018 990,150 +27%
2019 3,794 -100%
2020 812,160 +21308%
2021 338,979 -58%
2022 242,493 -28%
2023 647,506 +167%
2024 448,637 -31%

2024

Chemical Total (lbs) Air Water Land Off-Site
Formic acid
Diisocyanates 10,062
Certain glycol ethers
Methyl acrylate ♦ Carcinogen
Nitrate compounds (water dissociable; reportable only when in aqueous solution) 428,724 428,724 7,728
Toluene 9,863 9,863 963,871
Methanol 2,726 2,726 278,255
Xylene (mixed isomers) 1,838 1,838 221,098
Ethyl acrylate 1,836 1,836 413 ♦ Carcinogen
Cyclohexane 1,312 1,312 84,073
Dichloromethane 656 617 39 15,739 ♦ Carcinogen
n-Hexane 618 618 5,290
Acrylic acid 502 502 3,431
Ethylbenzene 179 179 2,960 ♦ Carcinogen
Butyl acrylate 174 174 587
Aluminum (fume or dust) 83 83 2,358
Phenol 68 1 67 16,015
Epichlorohydrin 38 38 2,074 ♦ Carcinogen
N,N-Dimethylformamide 17 17 9,294 ♦ Carcinogen
Lead compounds 2 2 113
Acrylamide 1 1 519 ♦ Carcinogen
Nitric acid 0 0 24,081
Mercury compounds 0 0 0 1

2023

Chemical Total (lbs) Air Water Land Off-Site
Potassium perfluorobutane sulfonate 693 PFAS
Certain glycol ethers
Propyleneimine ♦ Carcinogen
Aluminum (fume or dust)
Formic acid
Nitrate compounds (water dissociable; reportable only when in aqueous solution) 501,409 501,409 159
Sodium nitrite 78,090 78,090 68
Toluene 32,687 32,630 57 104,213
Methanol 21,904 21,903 1 290,207
Nitric acid 4,558 4,558 40,199
Ethyl acrylate 3,050 3,050 4,302 ♦ Carcinogen
Xylene (mixed isomers) 1,830 1,824 6 271,180
Dichloromethane 1,521 1,499 22 15,044 ♦ Carcinogen
Cyclohexane 979 979 46,507
n-Hexane 524 524 6,850
Acrylic acid 291 291 1,015
Butyl acrylate 279 279 308
Ethylbenzene 179 179 2,391 ♦ Carcinogen
Phenol 90 59 31 16,933
Methyl acrylate 43 43 795 ♦ Carcinogen
Nickel compounds 31 1 30 1,894 ♦ Carcinogen
Epichlorohydrin 17 17 4,133 ♦ Carcinogen
Chromium compounds (except for chromite ore mined in the Transvaal Region) 13 1 12 1,218
N,N-Dimethylformamide 6 6 7,654 ♦ Carcinogen
Lead compounds 5 1 3 319
Mercury compounds 0 0 0 37

2022

Chemical Total (lbs) Air Water Land Off-Site
Formic acid
Propyleneimine ♦ Carcinogen
Methyl acrylate ♦ Carcinogen
Butyl acrylate
Nitrate compounds (water dissociable; reportable only when in aqueous solution) 137,881 137,881 21
Sodium nitrite 42,650 42,650
Methanol 26,710 26,710 336,262
Toluene 19,293 19,285 9 107,971
Nitric acid 5,437 5,437 26,743
Dichloromethane 3,104 3,076 28 17,481 ♦ Carcinogen
Ethyl acrylate 2,870 2,870 272 ♦ Carcinogen
Xylene (mixed isomers) 1,481 1,465 16 287,497
Cyclohexane 1,260 1,260 44,187
n-Hexane 595 595 7,480
Phenol 285 89 196 2,352
Ethylbenzene 209 205 4 3,608 ♦ Carcinogen
Acrylic acid 192 192 1,492
Diisocyanates 165 165 4,247
Certain glycol ethers 145 145 3
Epichlorohydrin 86 86 4,113 ♦ Carcinogen
Aluminum (fume or dust) 77 77 253
Methyl isobutyl ketone 22 1 21 2,896 ♦ Carcinogen
N,N-Dimethylformamide 17 17 9,281 ♦ Carcinogen
Potassium perfluorobutane sulfonate 8 8 PFAS
Lead compounds 5 1 4 745
Mercury compounds 0 0 0

2021

Chemical Total (lbs) Air Water Land Off-Site
Poly[oxy(methyl-1,2-ethanediyl)], a-[2-[ethyl[(heptadecafluorooctyl)sulfonyl]amino]ethyl]-�-hydroxy- PFAS
Poly(oxy-1,2-ethanediyl), a-[2-[ethyl[(pentadecafluoroheptyl)sulfonyl]amino]ethyl]-�-methoxy- PFAS
2-[[(Heptadecafluorooctyl)sulfonyl]methylamino]ethyl acrylate PFAS
Poly(oxy-1,2-ethanediyl), a-hydro-�-hydroxy-, ether with a-fluoro-�-(2-hydroxyethyl)poly(difluoromethylene) (1:1) PFAS
Nitrate compounds (water dissociable; reportable only when in aqueous solution) 218,739 218,739
Sodium nitrite 59,157 59,157
Methanol 13,092 13,092 425,020
Toluene 13,051 13,044 7 55,615
Nitric acid 11,626 11,626 31
Vinyl acetate 3,134 3,134 1 ♦ Carcinogen
Ammonia 3,094 2,784 311 151
Xylene (mixed isomers) 2,564 2,564 283,316
Aluminum (fume or dust) 2,511 2,511
Ethyl acrylate 1,974 1,974 42 ♦ Carcinogen
Formaldehyde 1,781 214 1,567 3 ♦ Carcinogen
n-Hexane 1,496 1,496 978
Cyclohexane 1,324 1,324 6,932
Sulfuric acid (acid aerosols including mists, vapors, gas, fog, and other airborne forms of any particle size) 928 928
Methyl isobutyl ketone 874 865 9 29 ♦ Carcinogen
Butyl acrylate 581 581 50
Formic acid 555 555 2
Certain glycol ethers 365 365 1
Methyl tert-butyl ether 316 312 4 997
Hydrochloric acid (acid aerosols including mists, vapors, gas, fog, and other airborne forms of any particle size) 314 314
Ethylbenzene 294 294 95 ♦ Carcinogen
Acrylic acid 217 217 10
Lead compounds 153 5 148 523
Hydrogen fluoride 128 128 4
Phenol 120 32 88 11
tert-Butyl alcohol 90 90 17
Ethylene glycol 78 78 1,847
Methyl acrylate 75 75 ♦ Carcinogen
Chromium compounds (except for chromite ore mined in the Transvaal Region) 74 1 74 9,506
Trichloroethylene 58 58 ♦ Carcinogen
Dichloromethane 52 28 24 2,294 ♦ Carcinogen
Tetrachloroethylene 39 39 ♦ Carcinogen
Epichlorohydrin 29 29 ♦ Carcinogen
1-Chloro-1,1-difluoroethane (HCFC-142b) 26 26
Naphthalene 17 17 ♦ Carcinogen
N,N-Dimethylformamide 13 13 413 ♦ Carcinogen
N-Methyl-2-pyrrolidone 13 13 10
Acrylamide 12 12 0 ♦ Carcinogen
Propyleneimine 6 6 ♦ Carcinogen
Manganese compounds 5 5 14,232
Diisocyanates 3 3 12
Mercury compounds 2 2 0 0
Sulfluramid 1 1 PFAS
1-Octanesulfonamide, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-N-methyl- 1 1 PFAS
Acetonitrile 1 1
Toluene-2,4-diisocyanate 0 0 ♦ Carcinogen
Potassium perfluorooctanesulfonate 0 0 PFAS

2020

Chemical Total (lbs) Air Water Land Off-Site
1-Octanesulfonamide, N-butyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-N-(2-hydroxyethyl)- PFAS
2-[[(Heptadecafluorooctyl)sulfonyl]methylamino]ethyl acrylate PFAS
Tetrabromobisphenol A 577
Epichlorohydrin 25 ♦ Carcinogen
Poly(oxy-1,2-ethanediyl), a-hydro-�-hydroxy-, ether with a-fluoro-�-(2-hydroxyethyl)poly(difluoromethylene) (1:1) PFAS
Nitrate compounds (water dissociable; reportable only when in aqueous solution) 581,275 581,275 423
Sodium nitrite 157,455 157,455
Toluene 21,972 21,966 6 58,652
Methanol 20,723 20,723 124,524
Nitric acid 6,134 6,134 1,265
Formaldehyde 5,031 368 4,663 702 ♦ Carcinogen
Vinyl acetate 3,080 3,080 154 ♦ Carcinogen
Xylene (mixed isomers) 2,658 2,658 201,747
Ammonia 2,344 2,062 282
n-Hexane 1,224 1,224 760
Ethyl acrylate 1,196 1,196 101 ♦ Carcinogen
Methyl isobutyl ketone 1,188 1,186 2 826 ♦ Carcinogen
Sulfuric acid (acid aerosols including mists, vapors, gas, fog, and other airborne forms of any particle size) 1,108 1,108
Cyclohexane 1,091 1,091 847
Hydrochloric acid (acid aerosols including mists, vapors, gas, fog, and other airborne forms of any particle size) 831 831
Dichloromethane 814 810 4 16,628 ♦ Carcinogen
Certain glycol ethers 699 699 168,927
Formic acid 618 618 5,931
Butyl acrylate 514 514 4
Hydrogen fluoride 451 451 1,524
Methyl tert-butyl ether 398 397 1 31
Acrylic acid 259 259 176
Ethylbenzene 240 240 1,910 ♦ Carcinogen
Phenol 225 15 210 2,834
Lead compounds 135 4 131 1,028
Chromium compounds (except for chromite ore mined in the Transvaal Region) 66 9 57 14,095
Trichloroethylene 65 65 ♦ Carcinogen
Methyl acrylate 65 65 ♦ Carcinogen
tert-Butyl alcohol 58 58
Styrene 49 49 193 ♦ Carcinogen
Ethylene glycol 46 46 12
Tetrachloroethylene 44 44 ♦ Carcinogen
1-Chloro-1,1-difluoroethane (HCFC-142b) 33 33
N,N-Dimethylformamide 17 17 7,274 ♦ Carcinogen
N-Methyl-2-pyrrolidone 15 15 2,210
n-Butyl alcohol 11 11 447
Perfluorooctanoic acid 9 0 9 82 ♦ Carcinogen PFAS
Perfluorohexanesulfonic acid 6 6 115 PFAS
Diisocyanates 4 4 15
Acetonitrile 3 3 1
Perfluorooctane sulfonic acid 1 1 75 PFAS
Mercury compounds 1 1 0 12
Toluene-2,4-diisocyanate 1 1 1,326 ♦ Carcinogen
Acrylamide 1 1 1 ♦ Carcinogen
Sulfluramid 0 0 0 PFAS

2019

Chemical Total (lbs) Air Water Land Off-Site
Ammonia 2,010 1,695 315 34
Sulfuric acid (acid aerosols including mists, vapors, gas, fog, and other airborne forms of any particle size) 1,088 1,088
Ethylbenzene 209 209 5 ♦ Carcinogen
Lead compounds 139 11 128 951
Dichloromethane 131 109 22 122 ♦ Carcinogen
1-Chloro-1,1-difluoroethane (HCFC-142b) 79 79
N-Methyl-2-pyrrolidone 66 66
Manganese compounds 54 54 22,209
Acetonitrile 17 17
4,4'-Isopropylidenediphenol 0 0

2018

Chemical Total (lbs) Air Water Land Off-Site
Propyleneimine ♦ Carcinogen
Nitrate compounds (water dissociable; reportable only when in aqueous solution) 516,358 516,358 141
Sodium nitrite 373,521 373,521 6
Toluene 33,053 33,042 11 61,406
Methanol 29,752 29,752 174,808
Nitric acid 16,691 16,691 8,154
Xylene (mixed isomers) 3,867 3,867 356,135
Ammonia 2,109 1,827 282 2,052
Cyclohexane 1,861 1,861 4
Methyl isobutyl ketone 1,126 1,124 2 2 ♦ Carcinogen
n-Hexane 1,108 1,108 262
Hydrochloric acid (acid aerosols including mists, vapors, gas, fog, and other airborne forms of any particle size) 1,087 1,087
Formic acid 1,073 1,073
Sulfuric acid (acid aerosols including mists, vapors, gas, fog, and other airborne forms of any particle size) 938 938
Dichloromethane 936 878 58 64 ♦ Carcinogen
Ethyl acrylate 778 778 4 ♦ Carcinogen
Vinyl acetate 714 714 ♦ Carcinogen
Hydrogen fluoride 511 511 135
Certain glycol ethers 497 467 30 8,645
Formaldehyde 465 412 53 1,663 ♦ Carcinogen
Butyl acrylate 456 456
Manganese compounds 442 442 12,054
Ethylbenzene 425 425 1 ♦ Carcinogen
Methyl tert-butyl ether 255 254 1
Phenol 243 16 227 467
Acrylic acid 235 235
Zinc compounds 218 109 109 11,757
Ethylene glycol 189 189 1
Chromium compounds (except for chromite ore mined in the Transvaal Region) 188 127 61 14,095
Lead compounds 175 10 165 1,744
n-Butyl alcohol 156 156
Methyl acrylate 145 145 ♦ Carcinogen
1-Chloro-1,1-difluoroethane (HCFC-142b) 126 126
tert-Butyl alcohol 72 72
Styrene 64 64 8,288 ♦ Carcinogen
N,N-Dimethylformamide 45 45 ♦ Carcinogen
Trichloroethylene 43 43 ♦ Carcinogen
Diisocyanates 33 33 885
Acetonitrile 30 30
Tetrachloroethylene 30 30 ♦ Carcinogen
Chlorine 25 25 10
N-Methyl-2-pyrrolidone 22 22
2-Phenylphenol 21 21
4,4'-Methylenedianiline 12 12 ♦ Carcinogen
o-Xylene 10 10
Toluene-2,4-diisocyanate 8 8 173 ♦ Carcinogen
1,3-Phenylenediamine 7 7
4,4'-Isopropylidenediphenol 6 6 1
Epichlorohydrin 6 6 ♦ Carcinogen
2-Ethoxyethanol 5 5 5,540
Acrylamide 5 5 ♦ Carcinogen
1,2,4-Trimethylbenzene 4 4
p-Xylene 3 3
Mercury compounds 1 1 0 66
Mercury 1 1 0 67
Dioxin and dioxin-like compounds 0 0 ♦ Carcinogen

2017

Chemical Total (lbs) Air Water Land Off-Site
Nitrate compounds (water dissociable; reportable only when in aqueous solution) 551,753 551,753 56
Sodium nitrite 119,376 119,376 3
Toluene 26,337 26,332 5 56,497
Methanol 20,551 20,551 128,718
Nitric acid 18,733 18,733 51,385
Xylene (mixed isomers) 7,184 7,184 294,828
Methyl isobutyl ketone 4,999 4,996 3 5 ♦ Carcinogen
Vinyl acetate 4,906 4,906 63 ♦ Carcinogen
Methyl methacrylate 4,647 4,647
Ethyl acrylate 1,953 1,953 8 ♦ Carcinogen
Cyclohexane 1,932 1,932
Ammonia 1,750 1,650 100 470
Ethylene glycol 1,321 1,321 37,997
Hydrochloric acid (acid aerosols including mists, vapors, gas, fog, and other airborne forms of any particle size) 1,309 1,309
n-Hexane 1,157 1,157 155
Certain glycol ethers 942 942 19,161
Ethylbenzene 770 770 9 ♦ Carcinogen
Methyl tert-butyl ether 753 753
Acrylic acid 744 744 8
Sulfuric acid (acid aerosols including mists, vapors, gas, fog, and other airborne forms of any particle size) 732 732
Formaldehyde 568 497 71 ♦ Carcinogen
n-Butyl alcohol 550 550 8
Butyl acrylate 384 384
Lead compounds 382 11 371 1,565
Manganese compounds 366 366 35,905
Hydrogen fluoride 330 330 145
Formic acid 312 312
Zinc compounds 308 89 219 15,095
Methyl acrylate 260 260 ♦ Carcinogen
Phenol 252 43 209 4
1-Chloro-1,1-difluoroethane (HCFC-142b) 228 228
Trichloroethylene 227 227 ♦ Carcinogen
tert-Butyl alcohol 161 161
Tetrachloroethylene 152 152 ♦ Carcinogen
2-Ethoxyethanol 136 136
Chromium compounds (except for chromite ore mined in the Transvaal Region) 105 52 53 15,496
Dichloromethane 81 73 8 72 ♦ Carcinogen
N,N-Dimethylformamide 70 70 ♦ Carcinogen
Acetonitrile 63 63 2
Styrene 62 62 7,129 ♦ Carcinogen
N-Methyl-2-pyrrolidone 58 58
2-Phenylphenol 50 50
Naphthalene 31 31 ♦ Carcinogen
Diisocyanates 27 27 15,193
o-Xylene 24 24
p-Xylene 24 24
Chlorine 24 24
1,2,4-Trimethylbenzene 21 21
Acrylamide 14 14 ♦ Carcinogen
4,4'-Methylenedianiline 3 3 ♦ Carcinogen
Mercury compounds 2 2 0 29
1,3-Phenylenediamine 1 1
Ethylene oxide 1 1 ♦ Carcinogen

2016

Chemical Total (lbs) Air Water Land Off-Site
Tetrabromobisphenol A 169
Chlorine 289
4,4'-Methylenedianiline 61 ♦ Carcinogen
2-Phenylphenol 34
Propyleneimine ♦ Carcinogen
Benzoyl peroxide 333
Nitrate compounds (water dissociable; reportable only when in aqueous solution) 625,034 625,034
Sodium nitrite 211,198 211,198
Toluene 23,843 23,833 10 80,743
Methanol 18,373 18,373 144,507
Nitric acid 15,141 15,141 38,277
Xylene (mixed isomers) 6,272 6,272 281,576
Vinyl acetate 3,984 3,984 42 ♦ Carcinogen
Methyl isobutyl ketone 3,579 3,576 3 25 ♦ Carcinogen
Aluminum (fume or dust) 3,294 3,294 54,100
Phenol 3,011 57 2,954 1,072
Cyclohexane 2,234 2,234
Ammonia 1,906 1,790 117 821
Methyl methacrylate 1,864 1,864
Ethylene glycol 1,829 1,829
Sulfuric acid (acid aerosols including mists, vapors, gas, fog, and other airborne forms of any particle size) 1,582 1,582
n-Hexane 1,269 1,269 112
Acrylic acid 1,085 1,085 9
Certain glycol ethers 1,038 1,038 46,249
Dichloromethane 858 836 22 57 ♦ Carcinogen
Hydrochloric acid (acid aerosols including mists, vapors, gas, fog, and other airborne forms of any particle size) 811 811
Ethyl acrylate 789 789 2 ♦ Carcinogen
Ethylbenzene 721 721 158 ♦ Carcinogen
Zinc compounds 627 568 59 10,398
n-Butyl alcohol 554 554
Methyl tert-butyl ether 498 495 3
m-Xylene 497 497 2
Formaldehyde 489 441 48 3,835 ♦ Carcinogen
Manganese compounds 413 413 35,683
Hydrogen fluoride 343 343 384
Formic acid 339 339
Butyl acrylate 306 306
1-Chloro-1,1-difluoroethane (HCFC-142b) 254 254
Methyl acrylate 218 218 3 ♦ Carcinogen
Lead compounds 199 13 186 11,802
2-Ethoxyethanol 194 194 12,788
Trichloroethylene 188 188 ♦ Carcinogen
N,N-Dimethylformamide 175 175 ♦ Carcinogen
tert-Butyl alcohol 149 149
N-Methyl-2-pyrrolidone 140 140 1,098
Tetrachloroethylene 125 125 ♦ Carcinogen
Acetonitrile 117 117 2
o-Xylene 109 109 2
p-Xylene 108 108 2
Di(2-ethylhexyl) phthalate 106 15 91 18 ♦ Carcinogen
Nickel compounds 99 91 8 ♦ Carcinogen
Cobalt compounds 86 86 41,538 ♦ Carcinogen
Toluene-2,4-diisocyanate 70 70 5,703 ♦ Carcinogen
Triethylamine 67 67 3
Chromium compounds (except for chromite ore mined in the Transvaal Region) 60 15 45 13,555
Silver 51 51 310
Copper compounds 30 18 12 31
Allyl chloride 21 21
1,2,4-Trimethylbenzene 19 19
4,4'-Isopropylidenediphenol 14 14
Styrene 13 13 1,548 ♦ Carcinogen
Diisocyanates 10 10 100,942
Acrylamide 4 4 ♦ Carcinogen
Mercury compounds 1 1 0 90
1,3-Phenylenediamine 1 1
Dioxin and dioxin-like compounds 0 0 ♦ Carcinogen

2015

Chemical Total (lbs) Air Water Land Off-Site
4,4'-Methylenedianiline ♦ Carcinogen
Benzoyl peroxide
Cyanide compounds 22
Tetrabromobisphenol A
Acetonitrile 71
Acrylamide ♦ Carcinogen
Propyleneimine ♦ Carcinogen
o-Xylene 9
Sodium nitrite 414,696 414,696 831
Nitrate compounds (water dissociable; reportable only when in aqueous solution) 298,111 298,111 522
Toluene 22,294 22,288 6 49,034
Nitric acid 20,299 20,299 39,024
Methanol 19,251 19,251 143,737
Methyl isobutyl ketone 4,472 4,470 3 ♦ Carcinogen
Aluminum (fume or dust) 3,571 3,571 499
Vinyl acetate 3,423 3,423 303 ♦ Carcinogen
Cyclohexane 2,915 2,915 28
Antimony compounds 2,745 2,745 12,131
Formaldehyde 2,741 459 2,282 ♦ Carcinogen
Phenol 2,088 49 2,039 8
Ammonia 1,877 1,828 49 1,445
Xylene (mixed isomers) 1,795 1,795 245,503
Ethylene glycol 1,761 1,761
m-Xylene 1,245 1,245 9
n-Hexane 1,151 1,151 2,943
Sulfuric acid (acid aerosols including mists, vapors, gas, fog, and other airborne forms of any particle size) 1,041 1,041
Certain glycol ethers 1,014 1,014 29
Hydrochloric acid (acid aerosols including mists, vapors, gas, fog, and other airborne forms of any particle size) 836 836
Dichloromethane 750 657 93 69 ♦ Carcinogen
Acrylic acid 742 742
Ethylbenzene 681 681 1 ♦ Carcinogen
Methyl tert-butyl ether 599 598 1
Zinc compounds 530 484 46 7,756
Formic acid 439 439
Trichloroethylene 432 432 ♦ Carcinogen
Manganese compounds 426 426 37,403
n-Butyl alcohol 407 407
Ethyl acrylate 358 358 ♦ Carcinogen
1-Chloro-1,1-difluoroethane (HCFC-142b) 262 262 16,143
Methyl acrylate 245 245 ♦ Carcinogen
1,2-Dichloroethane 241 241 ♦ Carcinogen
Hydrogen fluoride 230 230 434
2-Ethoxyethanol 225 225
Butyl acrylate 157 157
Tetrachloroethylene 143 143 ♦ Carcinogen
tert-Butyl alcohol 131 131
Nickel compounds 105 95 10 13,402 ♦ Carcinogen
N-Methyl-2-pyrrolidone 99 99 3
Copper compounds 92 92 21,843
Cobalt compounds 90 90 35,700 ♦ Carcinogen
Chromium compounds (except for chromite ore mined in the Transvaal Region) 69 2 67 18,736
Methyl methacrylate 61 61
Styrene 57 57 ♦ Carcinogen
p-Xylene 41 41 9
Lead compounds 39 3 36 1,526
Diisocyanates 38 38
Barium compounds (except for barium sulfate (CAS No. 7727-43-7)) 29 29 29
Silver 15 15
N,N-Dimethylformamide 14 14 ♦ Carcinogen
Epichlorohydrin 11 11 ♦ Carcinogen
Chlorine 2 2
Mercury compounds 2 2 0 61
1,3-Phenylenediamine 1 1

Waste Management & Recycling

How this facility manages toxic chemicals beyond direct releases — through recycling, energy recovery, and on-site or off-site treatment. Data from the most recent TRI reporting year. Quantities in pounds.

Chemical Released Recycled Energy Recovery Treated
Nitrate compounds (water dissociable; reportable only when in aqueous solution) 1,160,727
Nitric acid 692
Diisocyanates 10,062
N,N-Dimethylformamide 9,294
Epichlorohydrin 2,074
Ethyl acrylate 1,198
Aluminum (fume or dust) 2,358
n-Hexane 579 4,711
Xylene (mixed isomers) 197,667 25,669
Dichloromethane 15,759
Methanol 70,280 208,120
Acrylamide 519
Phenol 16,015
Cyclohexane 49,525 34,575
Acrylic acid 3,431
Toluene 906,080 59,489
Butyl acrylate 587
Ethylbenzene 2,960

Off-Site Transfer Destinations

Facilities to which toxic chemicals were transferred for disposal, recycling, energy recovery, or treatment during the most recent TRI reporting year. Quantities in pounds.

Destination Chemical Disposal Recycling Energy Rec. Treatment
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Cyclohexane 1,572
CLEAN HARBORS DEER PARK
DEER PARK, TX
Cyclohexane 0
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Cyclohexane 0
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Cyclohexane 3,517
WRR ENVIRONMENTAL SERVICES CO INC
EAU CLAIRE, WI
Cyclohexane 49,525
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Ethylbenzene 2,517
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Ethylbenzene 0
CLEAN HARBORS DEER PARK
DEER PARK, TX
Ethylbenzene 0
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Ethylbenzene 443
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Dichloromethane 3,175
CLEAN HARBORS DEER PARK
DEER PARK, TX
Dichloromethane 0
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Dichloromethane 5,049
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Dichloromethane 7,514
CLEAN HARBORS LONE MOUNTAIN LLC
ORIENTA, OK
Dichloromethane 0
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
N,N-Dimethylformamide 0
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
N,N-Dimethylformamide 1,752
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
N,N-Dimethylformamide 7,542
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Acrylic acid 0
CLEAN HARBORS DEER PARK
DEER PARK, TX
Acrylic acid 1
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Acrylic acid 3,074
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Acrylic acid 0
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Aluminum (fume or dust) 0
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Aluminum (fume or dust) 2,305
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Aluminum (fume or dust) 53
CLEAN HARBORS DEER PARK
DEER PARK, TX
Methanol 907
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Methanol 15,454
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Methanol 168,366
WRR ENVIRONMENTAL SERVICES CO INC
EAU CLAIRE, WI
Methanol 70,280
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Methanol 23,248
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
n-Hexane 0
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
n-Hexane 1,061
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
n-Hexane 3,649
WRR ENVIRONMENTAL SERVICES CO INC
EAU CLAIRE, WI
n-Hexane 579
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Xylene (mixed isomers) 511
CLEAN HARBORS DEER PARK
DEER PARK, TX
Xylene (mixed isomers) 37
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Xylene (mixed isomers) 3,562
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Xylene (mixed isomers) 19,322
WRR ENVIRONMENTAL SERVICES CO INC
EAU CLAIRE, WI
Xylene (mixed isomers) 197,667
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Toluene 1
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Toluene 1,823
CLEAN HARBORS DEER PARK
DEER PARK, TX
Toluene 159
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Toluene 6,274
CLEAN HARBORS LONE MOUNTAIN LLC
ORIENTA, OK
Toluene 0
WRR ENVIRONMENTAL SERVICES CO INC
EAU CLAIRE, WI
Toluene 906,080
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Epichlorohydrin 0
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Epichlorohydrin 2,067
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Epichlorohydrin 7
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Ethyl acrylate 0
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Ethyl acrylate 192
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Ethyl acrylate 6
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Lead compounds 0
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Lead compounds 9
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Lead compounds 11
CLEAN HARBORS LONE MOUNTAIN LLC
ORIENTA, OK
Lead compounds 92
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Mercury compounds 0
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Mercury compounds 0
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Mercury compounds 0
CLEAN HARBORS LONE MOUNTAIN LLC
ORIENTA, OK
Mercury compounds 0
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Diisocyanates 0
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Diisocyanates 1,950
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Diisocyanates 8,112
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Phenol 619
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Phenol 15,395
CLEAN HARBORS LONE MOUNTAIN LLC
ORIENTA, OK
Phenol 0
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Phenol 1
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Nitrate compounds (water dissociable; reportable only when in aqueous solution) 41
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Nitrate compounds (water dissociable; reportable only when in aqueous solution) 7,629
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Nitrate compounds (water dissociable; reportable only when in aqueous solution) 58
CLEAN HARBORS LONE MOUNTAIN LLC
ORIENTA, OK
Nitrate compounds (water dissociable; reportable only when in aqueous solution) 0
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Nitric acid 61
CLEAN HARBORS DEER PARK
DEER PARK, TX
Nitric acid 10
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Nitric acid 54
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Nitric acid 567
SKB ROSEMOUNT INDUSTRIAL WASTE FACILITY
ROSEMOUNT, MN
Nitric acid 23,389
CLEAN HARBORS ARAGONITE, LLC
ARAGONITE, UT
Butyl acrylate 2
CLEAN HARBORS DEER PARK
DEER PARK, TX
Butyl acrylate 1
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Butyl acrylate 280
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Butyl acrylate 304
CLEAN HARBORS EL DORADO LLC
EL DORADO, AR
Acrylamide 389
CLEAN HARBORS ENVIRONMENTAL SERVICES INC
KIMBALL, NE
Acrylamide 131

Compliance Violations

Individual permit violations recorded by the EPA across air, water, and hazardous waste programs. Open violations are unresolved as of the most recent ECHO data update.

Program Type Violation Date Return to Compliance Status
caa FRV Nov 9, 2023 Open
rcra Standards Applicable to Generators of HW: General Nov 1, 2023 Mar 7, 2024 Resolved
rcra Standards Applicable to Generators of HW: Manifest Requirements Applicable to Small and Large Quantity Generators Nov 1, 2023 Mar 7, 2024 Resolved
rcra Standards for Owners and Operators of HW TSDs: General Facility Standards Sep 28, 2021 Open
rcra Standards Applicable to Recordkeeping and Reporting Applicable to Small and Large Quantity Generators Sep 28, 2021 Open
rcra Violation of a Federal or State Statute Sep 28, 2021 Open
rcra Standards Applicable to Generators of HW: General Sep 28, 2021 Open
rcra Standards for Owners and Operators of HW TSDs: Manifest System, Recordkeeping and Reporting Jan 12, 2021 Jul 5, 2022 Resolved
rcra Standards for Owners and Operators of HW TSDs: General Facility Standards Jan 12, 2021 Jul 5, 2022 Resolved
rcra Standards for Owners and Operators of HW TSDs: General Facility Standards Jan 4, 2021 Jul 5, 2022 Resolved
rcra Standards for Owners and Operators of HW TSDs: Manifest System, Recordkeeping and Reporting Jan 4, 2021 Jul 5, 2022 Resolved
rcra Standards for Owners and Operators of HW TSDs: Manifest System, Recordkeeping and Reporting Dec 16, 2020 Jul 5, 2022 Resolved
rcra Standards for Owners and Operators of HW TSDs: General Facility Standards Dec 16, 2020 Jul 5, 2022 Resolved
rcra Standards for Owners and Operators of HW TSDs: General Facility Standards Nov 2, 2020 Jul 5, 2022 Resolved
rcra Standards for Owners and Operators of HW TSDs: Manifest System, Recordkeeping and Reporting Nov 2, 2020 Jul 5, 2022 Resolved
rcra Standards for Owners and Operators of HW TSDs: General Facility Standards Sep 28, 2020 Jul 5, 2022 Resolved
rcra Standards for Owners and Operators of HW TSDs: General Facility Standards Jun 22, 2020 Jul 5, 2022 Resolved
caa FRV Aug 23, 2019 Open
rcra Standards Applicable to Generators of HW: General Sep 26, 2018 Jul 5, 2022 Resolved
rcra Standards for Owners and Operators of HW TSDs: General Facility Standards Sep 26, 2018 Jul 5, 2022 Resolved
rcra Standards for Used Oil: Generators Sep 26, 2018 Jul 5, 2022 Resolved
rcra Standards for Owners and Operators of HW TSDs: Preparedness and Prevention Sep 26, 2018 Jul 5, 2022 Resolved
cwa Effluent Violations - Unauthorized Discharge Aug 4, 2018 Open
cwa Effluent Violations - Unauthorized Discharge Jul 30, 2018 Open
cwa Effluent Violations - Industrial Spill Jun 15, 2018 Open
cwa Monitoring Violations - Improper Analysis or Lab Error Jun 20, 2016 Open
cwa Management Practice Violations - Best Management Practice Deficiencies Apr 30, 2015 Open
rcra Standards Applicable to Generators of HW: Pre-Transport Requirements Applicable to Small and Large Quantity Generators May 23, 2012 Apr 24, 2013 Resolved
rcra Standards for Owners and Operators of HW TSDs: Financial Requirements Oct 6, 2008 Jul 27, 2010 Resolved
rcra Standards for Owners and Operators of HW TSDs: Closure and Post-Closure Oct 6, 2008 Jul 27, 2010 Resolved
rcra Standards for Owners and Operators of HW TSDs: Use and Management of Containers May 28, 2008 Jul 27, 2010 Resolved
rcra Standards for Owners and Operators of HW TSDs: General Facility Standards May 28, 2008 Jul 27, 2010 Resolved
rcra Standards Applicable to Generators of HW: Pre-Transport Requirements Applicable to Small and Large Quantity Generators May 28, 2008 Jul 27, 2010 Resolved
rcra Standards for Owners and Operators of HW TSDs: Use and Management of Containers Oct 24, 2006 Feb 6, 2008 Resolved
rcra Standards Applicable to Generators of HW: General Aug 16, 2006 Mar 14, 2007 Resolved
rcra Standards Applicable to Generators of HW: General Aug 29, 2002 Jan 9, 2003 Resolved
rcra Standards Applicable to Generators of HW: Pre-Transport Requirements Applicable to Small and Large Quantity Generators Aug 29, 2002 Jan 9, 2003 Resolved
rcra Standards for Owners and Operators of HW TSDs: General Facility Standards Aug 29, 2002 Jan 9, 2003 Resolved
rcra Standards for Owners and Operators of HW TSDs: Air Emission Standards for Equipment Leaks Oct 27, 1998 Oct 11, 2000 Resolved
rcra Standards Applicable to Generators of HW: General Feb 17, 1997 Sep 11, 1997 Resolved
rcra Standards Applicable to Generators of HW: General Jun 12, 1996 Sep 20, 1996 Resolved
cwa Reporting Violations - Improper/ Incorrect Reporting Feb 28, 1994 Open
cwa Reporting Violations - Improper/ Incorrect Reporting Jan 31, 1994 Open
rcra Standards Applicable to Generators of HW: General Apr 29, 1993 Nov 1, 1993 Resolved
rcra Standards Applicable to Generators of HW: General Mar 23, 1993 Jun 17, 1993 Resolved
rcra Standards Applicable to Generators of HW: General Mar 14, 1991 Jun 21, 1991 Resolved
rcra Standards for Owners and Operators of HW TSDs: General Jan 31, 1990 May 24, 1990 Resolved
rcra Standards Applicable to Generators of HW: General Jun 9, 1989 Jul 20, 1990 Resolved
rcra Standards Applicable to Generators of HW: General May 30, 1989 Jul 20, 1990 Resolved
rcra Standards Applicable to Generators of HW: General Sep 14, 1988 Sep 14, 1988 Resolved

Discharge Limit Exceedances

Instances where this facility's reported discharge monitoring results exceeded its permitted limits under the Clean Water Act. Exceedance percentage shows how far over the permit limit the discharge was.

Pollutant Violation Reported Limit Exceedance Period Status
Mercury, total [as Hg] DMR, Limited - Numeric Violation 0.00 mg/L 0.00 +262% Dec 2025 Open
Chlorine, total residual DMR, Limited - Numeric Violation 0.04 mg/L 0.04 +5% Nov 2025 Open
Mercury, total [as Hg] DMR, Limited - Numeric Violation 0.00 mg/L 0.00 +105% Jun 2025 Open
Chlorine, total residual DMR, Limited - Numeric Violation 0.04 mg/L 0.00 +2,147,483,650% Sep 2024 Resolved
Chlorine, total residual DMR, Limited - Numeric Violation 0.09 mg/L 0.04 +125% Aug 2024 Open
BOD, 5-day, 20 deg. C DMR, Limited - Numeric Violation 68.00 mg/L 50.00 +36% Jul 2024 Open
Chlorine, total residual DMR, Limited - Numeric Violation 0.04 mg/L 0.00 +2,147,483,650% Jul 2024 Resolved
Solids, total suspended DMR, Limited - Numeric Violation 109.00 mg/L 45.00 +142% Jun 2024 Open
Chlorine, total residual DMR, Limited - Numeric Violation 0.04 mg/L 0.00 +2,147,483,650% May 2024 Resolved
Solids, total suspended DMR, Limited - Numeric Violation 1,490.00 kg/d 1,100.00 +35% May 2024 Open
Chlorine, total residual DMR, Limited - Numeric Violation 0.05 mg/L 0.04 +25% Dec 2023 Open
Oil and grease, hexane extr method DMR, Limited - Numeric Violation 12.00 mg/L 10.00 +20% Mar 2023 Open
BOD, 5-day, 20 deg. C DMR, Limited - Numeric Violation 69.00 mg/L 50.00 +38% Jan 2023 Open
Oil and grease, hexane extr method DMR, Limited - Numeric Violation 20.00 mg/L 10.00 +100% Apr 2022 Open
% of time exceeding pH limits DMR, Limited - Numeric Violation 1.32 % 1.00 +32% Jun 2021 Open
Zinc, total [as Zn] DMR, Limited - Numeric Violation 0.25 mg/L 0.24 +3% Jun 2019 Open
Chlorine, total residual DMR, Limited - Numeric Violation 0.03 mg/L 0.00 +2,147,483,650% May 2019 Open
Chlorine, total residual DMR, Limited - Numeric Violation 0.03 mg/L 0.00 +2,147,483,650% Aug 2018 Open
Temperature, water deg. fahrenheit DMR, Limited - Numeric Violation 87.00 deg F 83.00 +5% Jun 2018 Open
Chlorine, total residual DMR, Limited - Numeric Violation 0.01 mg/L 0.00 +2,147,483,650% Jul 2016 Open
Chlorine, total residual DMR, Limited - Numeric Violation 0.08 mg/L 0.04 +100% Jun 2016 Open
Chlorine, total residual DMR, Limited - Numeric Violation 0.01 mg/L 0.00 +2,147,483,650% Dec 2015 Open
Oil and grease, hexane extr method DMR, Limited - Numeric Violation 11.00 mg/L 10.00 +10% Dec 2015 Open
Chlorine, total residual DMR, Limited - Numeric Violation 0.01 mg/L 0.00 +2,147,483,650% Nov 2015 Open
Chlorine, total residual DMR, Limited - Numeric Violation 0.09 mg/L 0.00 +2,147,483,650% May 2015 Open
Chlorine, total residual DMR, Limited - Numeric Violation 0.03 mg/L 0.00 +2,147,483,650% Apr 2015 Open
Chlorine, total residual DMR, Limited - Numeric Violation 0.03 mg/L 0.00 +2,147,483,650% Jan 2015 Open

Enforcement Actions

Formal enforcement cases brought by the EPA or state agencies, including administrative orders and civil penalties assessed. Penalty amounts reflect what was formally assessed, not necessarily what was collected.

State CWA Penalty AO
Clean Water Act · Case MN-N00000551
$7,411
Warning Letter
Clean Air Act · Case 3604227657 · Dec 9, 2024
FINAL 3008(A) COMPLIANCE ORDER
RCRA (Hazardous Waste) · Case RCRA-MND006172969-001 · Feb 7, 2024
$4,165
Administrative - Formal
· Case 05-2023-5018 · Apr 6, 2023
$275,000
Notice of Violation
Clean Air Act · Case 3602180354 · Apr 8, 2020
State CWA Non Penalty AO
Clean Water Act · Case MN-NOV01032019 · Jan 3, 2019
Administrative - Formal
· Case 05-2017-5063 · Sep 29, 2017
$50,000
Administrative - Formal
· Case 05-2017-5052 · Sep 26, 2017
State CWA Non Penalty AO
Clean Water Act · Case MN-NOV 10312016 · Oct 31, 2016
Administrative - Formal
· Case 05-2014-5064 · Sep 25, 2014
$65,000
Notice of Violation (NOV)
RCRA (Hazardous Waste) · Case RCRA-MND006172969-019 · Feb 26, 2013
Administrative - Formal
· Case 05-2011-9104 · Aug 5, 2011
FORGIVEABLE & NON-FORGIVEABLE APO
RCRA (Hazardous Waste) · Case RCRA-MND006172969-018 · Jun 16, 2010
$8,611
Administrative - Formal
· Case HQ-2009-5024 · Sep 8, 2009
Administrative - Formal
· Case 05-2008-2706 · Jun 2, 2008
$30,000
Letter of Warning (LOW)
RCRA (Hazardous Waste) · Case RCRA-MND006172969-017 · Jan 19, 2007
Administrative - Formal
· Case 05-2004-0701 · Nov 14, 2003
Notice of Violation (NOV)
RCRA (Hazardous Waste) · Case RCRA-MND006172969-016 · Jan 9, 2003
State CWA Non Penalty AO
Clean Water Act · Case MN-N00000923 · Jun 5, 2002
Administrative - Formal
· Case HQ-2001-3005 · Jun 29, 2001

Other facilities in WASHINGTON County, MN

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